| Cryogenic implementation of charging diamond anvil cells with H(2) and D(2). | |
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MedLine Citation:
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PMID: 22047331 Owner: NLM Status: In-Data-Review |
Abstract/OtherAbstract:
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A cryogenic loading system for introducing H(2) and D(2) into the diamond anvil cell has been designed and constructed. The integration of pressure loading mechanism, ruby fluorescence spectrometer, and microscope camera allows for in situ tuning and calibrating the pressure. The performance of the system has been demonstrated by successful synthesis of hydride and deuteride of transition metal and rare earth metal. Our cryogenic methodology features facile start-over of loading and in situ electrical resistance measurement of as-synthesized sample. |
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Authors:
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Zhenhua Chi; Huyen Nguyen; Takahiro Matsuoka; Tomoko Kagayama; Naohisa Hirao; Yasuo Ohishi; Katsuya Shimizu |
Publication Detail:
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Type: Journal Article |
Journal Detail:
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Title: The Review of scientific instruments Volume: 82 ISSN: 1089-7623 ISO Abbreviation: Rev Sci Instrum Publication Date: 2011 Oct |
Date Detail:
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Created Date: 2011-11-03 Completed Date: - Revised Date: - |
Medline Journal Info:
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Nlm Unique ID: 0405571 Medline TA: Rev Sci Instrum Country: United States |
Other Details:
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Languages: eng Pagination: 105109 Citation Subset: IM |
Affiliation:
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KYOKUGEN, Center for Quantum Science and Technology under Extreme Conditions, Osaka University, Osaka 560-8531, JapanJapan Synchrotron Radiation Research Institute (JASRI)∕SPring-8, Hyogo 679-5198, Japan. |
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From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine
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