Document Detail


Comparison of methods and guaranteeing quality of analyses of urinary calculi--5th international ring test.
MedLine Citation:
PMID:  2800065     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
For five samples of our 5th international ring test for the quality control of methods of urinary calculus analysis we received 46 results from 19 countries obtained by means of ten different methods. The mean standard of quality (SQ) for all participants with quantitative methods is 2.11. Most laboratories employed X-ray diffraction (n = 21; SQ = 2.09) for quantitative calculus analysis. The mean deviation (delta x) per component from the ideal composition is fortunately low--about 0.10 molar parts for all participants, 0.06 molar parts for X-ray and infrared spectroscopy technique together. From the aspect of accuracy, the physical methods of analysis, X-ray diffraction and IR spectrophotometry, are clearly superior to all other analytical techniques.
Authors:
G Rebentisch; W Berg
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Publication Detail:
Type:  Comparative Study; Journal Article    
Journal Detail:
Title:  Urologia internationalis     Volume:  44     ISSN:  0042-1138     ISO Abbreviation:  Urol. Int.     Publication Date:  1989  
Date Detail:
Created Date:  1989-11-17     Completed Date:  1989-11-17     Revised Date:  2006-11-15    
Medline Journal Info:
Nlm Unique ID:  0417373     Medline TA:  Urol Int     Country:  SWITZERLAND    
Other Details:
Languages:  eng     Pagination:  298-302     Citation Subset:  IM    
Affiliation:
Central Laboratory, District Hospital of Cottbus, GDR.
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MeSH Terms
Descriptor/Qualifier:
Humans
Quality Control
Spectrophotometry, Infrared / standards
Urinary Calculi / analysis*
X-Ray Diffraction

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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