| Comparison of high-resolution solid-state NMR MQMAS and STMAS methods for half-integer quadrupolar nuclei. | |
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MedLine Citation:
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PMID: 17158036 Owner: NLM Status: MEDLINE |
Abstract/OtherAbstract:
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Several different amplitude-modulated two-dimensional high-resolution methods, based on MQMAS and STMAS, are compared. They include 3QMAS, 5QMAS, DQ-STMAS, and DQF-STMAS experiments. A new method, called t1-split-STMAS, is also proposed for spin-3/2 nuclei. The comparison is performed in terms of isotropic resolution and spectral-width, efficiency, and sensitivity to magic-angle offset and spinning speed fluctuations. |
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Authors:
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Julien Trebosc; Jean-Paul Amoureux; Zhehong Gan |
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Publication Detail:
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Type: Comparative Study; Evaluation Studies; Journal Article; Research Support, Non-U.S. Gov't Date: 2006-09-28 |
Journal Detail:
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Title: Solid state nuclear magnetic resonance Volume: 31 ISSN: 0926-2040 ISO Abbreviation: Solid State Nucl Magn Reson Publication Date: 2007 Feb |
Date Detail:
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Created Date: 2007-03-14 Completed Date: 2007-05-16 Revised Date: - |
Medline Journal Info:
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Nlm Unique ID: 9306181 Medline TA: Solid State Nucl Magn Reson Country: Netherlands |
Other Details:
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Languages: eng Pagination: 1-9 Citation Subset: IM |
Affiliation:
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UCCS, CNRS-8181, University of Lille-1, C7-ENSCL, 59652 Villeneuve d'Ascq, France. |
Export Citation:
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| MeSH Terms | |
Descriptor/Qualifier:
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Algorithms* Computer Simulation Magnetic Resonance Spectroscopy / methods* Models, Chemical* Models, Molecular* Reproducibility of Results Sensitivity and Specificity Signal Processing, Computer-Assisted* |
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