Document Detail


Clean-up and determination of sodium valproate in serum by high-performance liquid chromatography with fluorimetric detection.
MedLine Citation:
PMID:  1886916     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
A method is reported for the determination of the anticonvulsant sodium valproate in serum by fluorimetric detection. HPLC is performed on a reversed-phase column with a mobile phase of acetonitrile/water (65:35, v/v) with cyclohexane carboxylic acid as an internal standard. Samples were derivatized with 4-bromomethyl-7-methoxycoumarin and the optimized conditions are reported.
Authors:
E Bousquet; S Tirendi; N A Santagati; M Salvo; P Moncada Paterno Castello
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Die Pharmazie     Volume:  46     ISSN:  0031-7144     ISO Abbreviation:  Pharmazie     Publication Date:  1991 Apr 
Date Detail:
Created Date:  1991-10-07     Completed Date:  1991-10-07     Revised Date:  2007-01-29    
Medline Journal Info:
Nlm Unique ID:  9800766     Medline TA:  Pharmazie     Country:  GERMANY    
Other Details:
Languages:  eng     Pagination:  257-8     Citation Subset:  IM    
Affiliation:
Istituto di Chimica Farmaceutica e Tossicologica, Facoltá di Farmacia, Università di Catania, Italy.
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MeSH Terms
Descriptor/Qualifier:
Chromatography, High Pressure Liquid
Humans
Indicators and Reagents
Spectrometry, Fluorescence
Valproic Acid / blood*
Chemical
Reg. No./Substance:
0/Indicators and Reagents; 99-66-1/Valproic Acid

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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