Document Detail

Analysis of nitrofuran metabolites in food by high-performance liquid chromatography with tandem mass spectrometry detection.
MedLine Citation:
PMID:  14708885     Owner:  NLM     Status:  MEDLINE    
A reliable and sensitive procedure is presented for the analysis of nitrofuran metabolite residues in foods of animal origin, like poultry and shrimp. The method is based on a one-step extraction/derivatization, followed by solid-phase extraction clean-up with polymeric phase cartridges. The separations were carried out by liquid chromatography coupled with tandem mass spectroscopy detection. Results from the full validation of the procedure and from a survey of food available from the Swiss market, with the analysis of 236 samples of shrimp, poultry, fish and rabbit, are presented and demonstrate that this method is satisfactory in order to control nitrofuran residues in foods of animal origin.
Patrick Edder; Sandra Vargas; Didier Ortelli; Claude Corvi
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Clinical chemistry and laboratory medicine : CCLM / FESCC     Volume:  41     ISSN:  1434-6621     ISO Abbreviation:  Clin. Chem. Lab. Med.     Publication Date:  2003 Dec 
Date Detail:
Created Date:  2004-01-07     Completed Date:  2004-07-27     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  9806306     Medline TA:  Clin Chem Lab Med     Country:  Germany    
Other Details:
Languages:  eng     Pagination:  1608-14     Citation Subset:  IM    
Service de protection de la consommation, Genève, Switzerland.
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MeSH Terms
Chromatography, High Pressure Liquid / methods*
Food Analysis*
Nitrofurans / analysis*
Spectrometry, Mass, Electrospray Ionization / methods*
Reg. No./Substance:

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