| 4,4'-Bipyridine-3-nitro-benzoic acid (1/2). | |
| | |
MedLine Citation:
|
PMID: 21580317 Owner: NLM Status: PubMed-not-MEDLINE |
Abstract/OtherAbstract:
|
The title compound, C(10)H(8)N(2)·2C(7)H(5)NO(4),was obtained unintentionally as the harvested product of the hydro-thermal reaction between Co(OAc)(2)·4H(2)O and 4,4'-bipyridine in the presence of 3-nitro-phthalic acid. In the reaction, 3-nitro-phthalic acid is transformed into 3-nitro-benzoic acid by an in situ deca-rboxylation reaction, in which the carboxyl-ate group is not deprotonated and is uncoordinated. In the crystal, the uncoordinated 3-nitro-benzoic acid and free 4,4'-bipyridine mol-ecules are linked alternately by O-H⋯N hydrogen bonds into chains, which are assembled by C-H⋯O hydrogen bonds into a three-dimensional supra-molecular network. |
| | |
Authors:
|
Zhen Zhu; Feng-Qin Wang; Yong-Nan Zhao |
Related Documents
:
|
7357247 - The effect of bile salts on the pancreatic duct mucosal barrier. 6768777 - Action of rennin on casein. iii. effect of alpha s- and beta-casein on the secondary ph... 23489367 - Hepatic triacylglycerol synthesis and secretion: dgat2 as the link between glycaemia an... 6262477 - Analytical determination of purity of 1-piperidinocyclohexanecarbonitrile and its hydro... 11510907 - Serum acid phosphatase as a tumour marker in giant cell tumour of bone. 9684157 - Production of gamma-aminobutyric acid by cheese starters during cheese ripening. |
Publication Detail:
|
Type: Journal Article Date: 2010-02-06 |
Journal Detail:
|
Title: Acta crystallographica. Section E, Structure reports online Volume: 66 ISSN: 1600-5368 ISO Abbreviation: Acta Crystallogr E Struct Rep Online Publication Date: 2010 |
Date Detail:
|
Created Date: 2011-05-17 Completed Date: 2011-07-14 Revised Date: 2011-11-11 |
Medline Journal Info:
|
Nlm Unique ID: 101089178 Medline TA: Acta Crystallogr E Struct Rep Online Country: England |
Other Details:
|
Languages: eng Pagination: o546 Citation Subset: - |
Export Citation:
|
APA/MLA Format Download EndNote Download BibTex |
| MeSH Terms | |
Descriptor/Qualifier:
|
|
| Comments/Corrections | |
From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine
Previous Document: 2,4-Bis(4-chloro-phen-yl)-1-methyl-3-aza-bicyclo-[3.3.1]nonan-9-one.
Next Document: 12-(4-Chloro-phen-yl)-9,9-dimethyl-9,10-dihydro-8H-benzo[a]xanthen-11(12H)-one.