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2-(5-Bromo-pyridin-3-yl)-5-[3-(4,5,6,7-tetra-hydro-thieno[3,2-c]pyridine-5-ylsulfon-yl)thio-phen-2-yl]-1,3,4-oxa-diazole.
MedLine Citation:
PMID:  22058804     Owner:  NLM     Status:  PubMed-not-MEDLINE    
Abstract/OtherAbstract:
In the title compound, C(18)H(13)BrN(4)O(3)S(3), the tetra-hydro-pyridine ring adopts a half-chair conformation with the central methyl-ene-C atom of the NCH(2)CH(2) unit at the flap. The dihedral angles between the tetra-hydro-pyridine ring and the pyridine and two thio-phene rings are 69.34 (13) 5.66 (13) and 68.63 (13)°, respectively, while the dihedral angle between the 1,3,4-oxadiazole and tetra-hydro-pyridine rings is 54.76 (13)°. The mol-ecule is stabilized by an intra-molecular C-H⋯N inter-action. In the crystal, adjacent mol-ecules are connected via bifurcated C-H⋯(N,O) hydrogen bonds, forming a chain along the b axis.
Authors:
Hoong-Kun Fun; Madhukar Hemamalini; Sankappa Rai; A M Isloor; Prakash Shetty
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Publication Detail:
Type:  Journal Article     Date:  2011-09-30
Journal Detail:
Title:  Acta crystallographica. Section E, Structure reports online     Volume:  67     ISSN:  1600-5368     ISO Abbreviation:  Acta Crystallogr Sect E Struct Rep Online     Publication Date:  2011 Oct 
Date Detail:
Created Date:  2011-11-07     Completed Date:  2011-11-10     Revised Date:  2011-12-09    
Medline Journal Info:
Nlm Unique ID:  101089178     Medline TA:  Acta Crystallogr Sect E Struct Rep Online     Country:  England    
Other Details:
Languages:  eng     Pagination:  o2743-4     Citation Subset:  -    
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